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1 article(s) from Mokbel, Haifaa

Towards new NIR dyes for free radical photopolymerization processes

Haifaa Mokbel,
Guillaume Noirbent,
Didier Gigmes,
Frédéric Dumur and
Jacques Lalevée

Beilstein J. Org. Chem. 2021, 17, 2067–2076, doi:10.3762/bjoc.17.133

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Graphical Abstract

Scheme 1: Investigated NIR dyes.

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Scheme 2: Other used chemicals.

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Scheme 3: Synthetic routes to compounds Ca, Cb, and CNa.

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Scheme 4: Synthetic routes to CI1, CI3, CI4, and CI6–CI9.

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Scheme 5: The metathesis reaction enabling the formation of “soft” salts CBPh1-CBPh4.

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Figure 1: Visible–NIR spectra of NIR dyes in ACN. A) (1) CBPh1, (2) CBPh2, (3) CBPh3, (4) CBPh4, (5) Ca, (6) ...

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Figure 2: Photopolymerization profiles of PETIA monomer under air (acrylate functions conversion vs irradiati...

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Figure 3: Photopolymerization profiles of PETIA monomer under air (acrylate functions conversion vs irradiati...

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Scheme 6: Pictures of polymers obtained for a thickness of 1.4 mm, using a NIR dye/iod/amine 0.1:3:2, %w/w/w ...

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Scheme 7: Proposed mechanism for the photochemical reactivity of NIR dyes in a three-component PIS.

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Figure 4: A) Photopolymerization profiles of PETIA/epoxy blend 1:1, w/w under air (acrylate and epoxy functio...

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Published 16 Aug 2021

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